Registration Dossier
Registration Dossier
Please be aware that this old REACH registration data factsheet is no longer maintained; it remains frozen as of 19th May 2023.
The new ECHA CHEM database has been released by ECHA, and it now contains all REACH registration data. There are more details on the transition of ECHA's published data to ECHA CHEM here.
Use of this information is subject to copyright laws and may require the permission of the owner of the information, as described in the ECHA Legal Notice.
EC number: 447-920-2 | CAS number: 897393-42-9
Boiling point
Administrative data
Link to relevant study record(s)
- Endpoint:
- boiling point
- Type of information:
- experimental study
- Adequacy of study:
- key study
- Study period:
- 08 May 2003
- Reliability:
- 1 (reliable without restriction)
- Rationale for reliability incl. deficiencies:
- guideline study
- Qualifier:
- according to guideline
- Guideline:
- EU Method A.2 (Boiling Temperature)
- Qualifier:
- according to guideline
- Guideline:
- OECD Guideline 103 (Boiling point/boiling range)
- GLP compliance:
- yes
- Type of method:
- differential scanning calorimetry
- Specific details on test material used for the study:
- - Batch: 8191-34
- Purity: 97.8% (expressed as primary amine, % of total) - Key result
- Decomposition:
- yes
- Decomp. temp.:
- >= 148 °C
- Remarks on result:
- other: Atmospheric pressure was not reported; ambient conditions are anticipated.
- Conclusions:
- The test substance starts to decompose at 148 °C under ambient conditions.
Reference
The DSC curves showed a small exothermic effect (onset at 148 - 150 °C) probably caused by a reaction or decomposition; the substance changed from clear colourless to light yellow.
Under further heating a sharp endothermic peak (onset at 260 - 270 °C) was observed, probably caused by evaporation of the substance. The extrapolated onset temperature (280 - 282 °C) could be concluded to be the boiling temperature; however as discoloration of the substance had already occurred at a lower temperature, this should be regarded as the boiling temperature of the reacted and/or decomposed substance.
A further significant exothermic reaction occurred immediately after the endothermic reaction indicating further reaction and / or decomposition which is confirmed by a loss of sample weight (85 - 98%) and a further coloration (to brown).
Description of key information
In a GLP study according to test methods EC A.2 and OECD 103 (differential scanning calorimetry), the substance was determined to decompose at and above 148°C (Van der Baan-Treur, 2003).
Key value for chemical safety assessment
Additional information
The substance was concluded to decompose before its boiling temperature.
Information on Registered Substances comes from registration dossiers which have been assigned a registration number. The assignment of a registration number does however not guarantee that the information in the dossier is correct or that the dossier is compliant with Regulation (EC) No 1907/2006 (the REACH Regulation). This information has not been reviewed or verified by the Agency or any other authority. The content is subject to change without prior notice.
Reproduction or further distribution of this information may be subject to copyright protection. Use of the information without obtaining the permission from the owner(s) of the respective information might violate the rights of the owner.
