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Reference
Endpoint:
relative self-ignition temperature (solids)
Type of information:
experimental study
Adequacy of study:
key study
Study period:
23 February 2017 to 01 March 2017
Reliability:
1 (reliable without restriction)
Rationale for reliability incl. deficiencies:
guideline study
Reason / purpose for cross-reference:
reference to same study
Qualifier:
according to guideline
Guideline:
EU Method A.16 (Relative Self-Ignition Temperature for Solids)
Version / remarks:
2008
Deviations:
no
GLP compliance:
yes (incl. QA statement)
Specific details on test material used for the study:
SOURCE OF TEST MATERIAL
- Batch No.of test material: PR203-4/16
- Expiration date of the lot/batch: 21 December 2017

STABILITY AND STORAGE CONDITIONS OF TEST MATERIAL
- Storage condition of test material: Room temperature over silica gel, under nitrogen in the dark

Key result
Relative self-ignition temperature:
> 400 °C
Remarks on result:
no self ignition observed under the test conditions

The test material was a pale green powdery solid. Whilst heating the test material, no significant exothermic reaction/self-heating of the sample was observed. On completion of the test, the test material was a pale green powder with some black charring.

Conclusions:
Under the conditions of the study, the test material has been determined not to have a relative self-ignition temperature below 400 °C.
Executive summary:

The relative self ignition temperature of the test material was determined in accordance with the standardised guideline EU Method A.16 under GLP conditions.

The test material was a pale green powdery solid. Whilst heating the test material from ambient to 400°C at a rate of 0.5°C/min, no significant exothermic reaction/self-heating of the sample was observed. On completion of the test, the test material was a pale green powder with some black charring.

Under the conditions of the study, the test material has been determined not to have a relative self-ignition temperature below 400°C.

Description of key information

Under the conditions of the study, the test material has been determined not to have a relative self-ignition temperature below 400°C.

Key value for chemical safety assessment

Additional information

The relative self ignition of the test material was determined in accordance with the standardised guideline EU Method A.16 under GLP conditions. The study was awarded a reliability score of 1 in accordance with the criteria set forth by Klimisch et al. (1997).

The test material was a pale green powdery solid. Whilst heating the test materialfrom ambient to 400°C at a rate of 0.5°C/min, no significant exothermic reaction/self-heating of the sample was observed. On completion of the test, the test material was a pale green powder with some black charring.

Under the conditions of the study, the test material has been determined not to have a relative self-ignition temperature below 400°C.