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Physical & Chemical properties

Boiling point

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Administrative data

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Reference
Endpoint:
boiling point
Type of information:
experimental study
Adequacy of study:
key study
Study period:
2007-07-04 - 2007-07-12
Reliability:
1 (reliable without restriction)
Rationale for reliability incl. deficiencies:
guideline study
Qualifier:
according to guideline
Guideline:
EU Method A.2 (Boiling Temperature)
Version / remarks:
92/69/EEC
Deviations:
no
Qualifier:
according to guideline
Guideline:
OECD Guideline 103 (Boiling Point)
Version / remarks:
1995
Deviations:
no
GLP compliance:
no
Type of method:
differential scanning calorimetry
Key result
Boiling pt.:
>= 405 - <= 455 °C
Atm. press.:
ca. 1 013.25 hPa
Decomposition:
no

Three measurements in aluminium crucibles with a hole showed an endothermic effect after melting in


the temperature range 405 -455 °C with an onset temperature of 440 °C.


 


 


Table 1: Boiling Point (DSC measurement).







































Ident No.



Starting temperature / °C



Final test temperature / °C



Temperature range (boiling) / °C



Onset / °C



Crucible



26398



25



500



405-455



439.0



Aluminium with a hole



26400



25



500



405-455


 



442.23



Aluminium with a hole



26401



25



500



410-470



441.02



Aluminium with a hole




 


The test item had a boiling range at atmospheric pressure of 405 -455 °C

Conclusions:
The test item had a boiling range at atmospheric pressure of 405- 455 °C.
Executive summary:

A study was conducted according to OECD test guideline 103 and Regulation (EC) No 440/2008 method A.2 to determine the boiling point of the test item using differential scanning calorimetry (DSC 25 -500 °C). The test item and the reference are heated up from the starting temperature to the final temperature at a constant heating rate in a defined atmosphere (nitrogen). Open crucibles are used as containers for the test item and as empty reference crucible. The quantity of heat absorbed or released is measured and recorded. The test item had a boiling range at atmospheric pressure of 405- 455 °C.

Description of key information

The test item had a boiling range at atmospheric pressure of 405 -455 °C.

Key value for chemical safety assessment

Additional information

A study was conducted according to OECD test guideline 103 and Regulation (EC) No 440/2008 method A.2 to determine the boiling point of the test item using differential scanning calorimetry (DSC 25 -500 °C). The test item and the reference are heated up from the starting temperature to the final temperature at a constant heating rate in a defined atmosphere (nitrogen). Open crucibles are used as containers for the test item and as empty reference crucible. The quantity of heat absorbed or released is measured and recorded. The test item had a boiling range at atmospheric pressure of 405- 455 °C.