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Please be aware that this old REACH registration data factsheet is no longer maintained; it remains frozen as of 19th May 2023.

The new ECHA CHEM database has been released by ECHA, and it now contains all REACH registration data. There are more details on the transition of ECHA's published data to ECHA CHEM here.

Diss Factsheets

Administrative data

Endpoint:
melting point/freezing point
Type of information:
experimental study
Adequacy of study:
key study
Study period:
2021
Reliability:
1 (reliable without restriction)

Data source

Reference
Reference Type:
study report
Title:
Unnamed
Year:
2021
Report date:
2021

Materials and methods

Test guideline
Qualifier:
according to guideline
Guideline:
OECD Guideline 102 (Melting point / Melting Range)
GLP compliance:
no
Type of method:
capillary method

Test material

Constituent 1
Reference substance name:
Docosan-1-ol, icosan-1-ol, octadecan-1-ol and their reaction products with betaine and ethanesulphonic acid
IUPAC Name:
Docosan-1-ol, icosan-1-ol, octadecan-1-ol and their reaction products with betaine and ethanesulphonic acid
Test material form:
solid: bulk

Results and discussion

Melting / freezing point
Melting / freezing pt.:
70.63 °C
Atm. press.:
1 020.3 hPa

Applicant's summary and conclusion

Executive summary:

Test system


    Capillary tube in a metal block


Stuart SMP30.


     Preparation


The samples of the three batches are put into capillary tubes fused at one end. To obtain a uniformly packed sample, the capillary tubes are dropped from a height onto a watch glass.


     Measurement


The three capillary tubes, filled with the samples, are placed in a heated metal block. The temperature is raised up to 60°C and once it is reached, it is stabilized for 120 s. Then the metal block is heated so that the temperature rise is 5°C/min.


Results
























 



Batch P20843



Batch P20517



Batch P21096



Beginning of melting (°C)



70,3



70,0



71,6



Final stage of melting (°C)



73,5



73,4



74,9