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Diss Factsheets

Administrative data

Endpoint:
melting point/freezing point
Type of information:
experimental study
Adequacy of study:
key study
Study period:
2003
Reliability:
1 (reliable without restriction)
Rationale for reliability incl. deficiencies:
guideline study

Data source

Reference
Reference Type:
study report
Title:
Unnamed
Year:
2003
Report date:
2003

Materials and methods

Test guidelineopen allclose all
Qualifier:
according to guideline
Guideline:
OECD Guideline 102 (Melting point / Melting Range)
Deviations:
no
Qualifier:
according to guideline
Guideline:
EU Method A.1 (Melting / Freezing Temperature)
Deviations:
no
GLP compliance:
yes (incl. QA statement)
Type of method:
differential scanning calorimetry

Test material

Constituent 1
Chemical structure
Reference substance name:
-
EC Number:
453-090-2
EC Name:
-
Cas Number:
140456-78-6
Molecular formula:
NH4 N(NO2)2
IUPAC Name:
Ammonium dinitroazanide
Test material form:
solid: particulate/powder
Specific details on test material used for the study:
Batch 2003 7026

Results and discussion

Melting / freezing point
Melting / freezing pt.:
93.2 °C
Atm. press.:
1 atm

Any other information on results incl. tables

A preliminary DSC-test (20 K/min) lead to the observation of a peak at 93.2 °C. A second, more precise (5 K/min) test confirmed the result of 93.2 °C.

Applicant's summary and conclusion

Conclusions:
The melting point of the substance is 93.2°C.