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Physical & Chemical properties

Melting point / freezing point

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Reference
Endpoint:
melting point/freezing point
Type of information:
experimental study
Adequacy of study:
key study
Reliability:
1 (reliable without restriction)
Rationale for reliability incl. deficiencies:
guideline study
Qualifier:
according to guideline
Guideline:
OECD Guideline 102 (Melting point / Melting Range)
Version / remarks:
adopted on 27 July 1995
Deviations:
no
Qualifier:
according to guideline
Guideline:
EU Method A.1 (Melting / Freezing Temperature)
Version / remarks:
2008
Deviations:
no
GLP compliance:
no
Type of method:
other: determined by differential scanning calorimetry and visual methods
Melting / freezing pt.:
>= -26.9 - <= 9 °C
Atm. press.:
1 015 hPa
Remarks on result:
other: pour point: 5 °C ± 3 °C
Conclusions:
The melting temperature of the test item was determined by differential scanning calorimetry and visual methods according to the OECD Test Guideline 102 and EU test method A.1:
Melting Range: -26.9 °C - 9.0 °C (1015 hPa)
Pour Point 5 °C ± 3 °C
Executive summary:

The melting temperature of polyglycerin caprylate/caprinate was determined by differential scanning calorimetry and visual methods according to the OECD Test Guideline 102 and EU test method A.1.

No abrupt change of the physical state at a specific temperature was observed, but a continuously increasing viscosity of the sample. The lowest temperature at which movement could be observed was 5 °C ± 3 °C (pour point).

By means of DSC an average melting range of -26.9 °C - 9 °C was measured which is in accordance with the liquefaction measured by visual observation in the melt microscope.

Description of key information

The melting temperature of polyglycerin caprylate/caprinate was determined by differential scanning calorimetry and visual methods according to the OECD Test Guideline 102 and EU test method A.1.

No abrupt change of the physical state at a specific temperature was observed, but a continuously increasing viscosity of the sample. The lowest temperature at which movement could be observed was 5 °C ± 3 °C (pour point).

By means of DSC an average melting range of -26.9 °C - 9 °C was measured which is in accordance with the liquefaction measured by visual observation in the melt microscope.

Key value for chemical safety assessment

Melting / freezing point at 101 325 Pa:
5 °C

Additional information